摘要: |
研究了食品用密封圈正己烷蒸发残渣量与样品的浸泡方法、截取方式、横切面数量、回流温度和冷凝回流完成后的处理等的关系,结果表明,浸泡方法、回流温度和冷凝回流完成后的处理等因素对蒸发残渣量影响明显,且蒸发残渣量随着横切面的增加而增大。研究影响因素的同时,给出了试验中每个环节的控制指标,保证了检验结果的可重复性和真实性。 |
关键词: 蒸发残渣 正己烷 横切面 质量法 回流温度 |
DOI: |
分类号:TB484.3; TB487 |
基金项目: |
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Study of Influencing Factors on Evaporation Residue of Food-contact N-hexane Obturating Ring |
ZHANG Zhi-li, WANG Wei-shan, XU Chao, SHEN Li-xia, ZHANG Qian
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Shandong Supervision and Inspection Institute for Product Quality, Jinan 250103, China
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Abstract: |
The relation between evaporation residue of food-contact n-hexane obturating ring and treatment parameters, which included soak method, cut method, number of cross-section, reflux temperature, and treatment after condensation, was analyzed. The results showed that soak method, reflux temperature, and treatment after condensation are main influencing factors; evaporation residue amount increases with increasing cross-section. The control levels in each sector of inspection process were put forward to ensure repeatability and authenticity of inspection result. |
Key words: evaporation residue n-hexane cross-section mass method reflux temperature |